Browsing Artículos-Grupo de investigación IMaCris / MaKrisI by Author "Serrano Larrea, Edurne"
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Catalytic Performance of a New 1D Cu(II) Coordination Polymer {Cu(NO3)(H2O)}(HTae)(4,40-Bpy) for Knoevenagel Condensation
Serrano Larrea, Edurne; Fernández de Luis, Roberto; Arriortua Marcaida, María Isabel (MDPI, 2016-12-01)The {Cu(NO3)(H2O)}(HTae)(4,40-Bpy) (H2Tae = 1,1,2,2-tetraacetylethane, 4,40-Bpy = 4,40-Dipyridyl) 1D coordination polymer has been obtained by slow evaporation. The crystal structure consists of parallel and oblique ... -
Crystal structure of K0.75[FeII 3.75FeIII 1.25(HPO3)6]- 0.5H2O, an open-framework iron phosphite with mixed-valent FeII/FeIII ions
Serrano Larrea, Edurne; Mesa Rueda, José Luis; Legarra Sáez, Estíbaliz ; Aguayo Urquijo, Andrés Tomás ; Arriortua Marcaida, María Isabel (International Union of Crystallography, 2016)Single crystals of the title compound, potassium hexaphosphitopentaferrate( II,III) hemihydrate, K0.75[FeII 3.75FeIII 1.25(HPO3)6] 0.5H2O, were grown under mild hydrothermal conditions. The crystal structure is isotypic ... -
Encapsulation of β-alanine model amino-acid in zirconium(IV) metal organic frameworks: Defect engineering to improve host guest interactions
Rodríguez Muguruza, Asier; Fernández de Luis, Roberto; Iglesias, Naroa; Bazán Blau, Begoña del Pilar ; Urtiaga Greaves, Miren Karmele ; Serrano Larrea, Edurne; Fidalgo Marijuan, Arkaitz; Barandika Argoitia, Miren Gotzone (Elsevier, 2020-04)Metal-Organic Frameworks (MOFs) are porous coordination networks assembled through metal complexes with organic linkers. Due to their chemical versatility, these materials are being investigated for various applications ... -
Heterogeneous catalytic properties of unprecedented m-O-[FeTCPP]2 dimers (H2TCPP = meso-tetra(4-carboxyphenyl)porphyrin): unusual superhyperfine EPR structure
Fidalgo Marijuan, Arkaitz; Barandika Argoitia, Miren Gotzone ; Bazán Blau, Begoña del Pilar ; Urtiaga Greaves, Miren Karmele ; Serrano Larrea, Edurne; Iglesias, Marta; Lezama Diago, Luis María; Arriortua Marcaida, María Isabel (RSC Publishing, 2015-01-07)During the past years, a great effort has been devoted to the anchoring of catalysts into solid coordination networks in order to achieve heterogeneous catalysts. In this sense, an innovative approach consists on using the ... -
Hydrothermal Synthesis and Study of Inorganic-Organic Hybrid Vanadate of Nickel(II) Coordination Complex with Pyrazine, Ni3(C4H4N2)3(V8O23)
Serrano Larrea, Edurne; Mesa Rueda, José Luis; Arriortua Marcaida, María Isabel (Elsevier, 2011-02-25)The three-dimensional hybrid compound Ni3(C4H4N2)3(V8O23) has been synthesized by mild hydrothermal methods under autogenous pressure at 170 ºC, together with another hybrid phase, Ni2(C4H4N2)(V4O12)(H2O)2. The isolation ... -
M(C6H16N3)2(VO3)4 as heterogeneous catalysts. Study of three new hybrid vanadates of cobalt(II), nickel(II) and copper(II) with 1-(2-aminoethyl)piperazonium.
Serrano Larrea, Edurne; Mesa Rueda, José Luis; Pizarro Sanz, José Luis ; Iglesias, Marta; Rojo Aparicio, Teófilo ; Arriortua Marcaida, María Isabel (Royal Society of Chemistry, 2011-10-14)Three new hybrid vanadates have been synthesized under hydrothermal conditions with the formula M(C6H16N3)2(VO3)4, where M= Co(II), Ni(II) and Cu(II). The structural analyses show that the phases are isostructural and ... -
Mild Hydrothermal Synthesis, Crystal Structure, Thermal Behavior, Spectroscopic and Magnetic Properties of (NH4)0.80Li0.20[Fe(AsO4)F]
Berrocal Torres, Teresa; Mesa Rueda, José Luis; Serrano Larrea, Edurne; Bazán Blau, Begoña del Pilar ; Pizarro Sanz, José Luis ; Lezama Diago, Luis María; Rojo Aparicio, Teófilo ; Arriortua Marcaida, María Isabel (Elsevier, 2011-08-03)The (NH4)0.80Li0.20[Fe(AsO4)F] compound has been synthesized under mild hydrothermal conditions. The compound crystallize in the orthorhombic Pna21 space group, with cell parameters a= 13.352(9), b= 6.7049(9), c= 10.943(2) ... -
Open and closed forms of the interpenetrated [Cu2(Tae)(Bpa)2](NO3)2•nH2O cationic coordination polymer: magnetic properties and high pressure CO2/CH4 gas sorption.
Fernández de Luis, Roberto; Serrano Larrea, Edurne; Orive Gómez de Segura, Joseba; Fidalgo Marijuan, Arkaitz; Lezama Diago, Luis María; Arriortua Marcaida, María Isabel (The Royal Society of Chemistry, 2018-01-21)Two closed and one open structural forms of the interpenetrated [Cu2(Tae)(Bpa)2](NO3)2•nH2O (H2Tae= 1,1,2,2-tetraacetylethane, Bpa= 1,2-Bis(4-pyridyl)ethane) cationic coordination polymer have been synthesized. Three ... -
Structural Transformations in the Thermal Dehydration of [Cu2(bpa)(btec)(H2O)4]n Coordination Polymer
Bravo García, Laura ; Serrano Larrea, Edurne; Artetxe Arretxe, Beñat; Lezama Diago, Luis María; Gutiérrez Zorrilla López, Juan Manuel ; Arriortua Marcaida, María Isabel (MDPI, 2019-05-13)Reactions between pyridinic ligands such as 1,2-bis(4-pyridyl)ethane (bpa) and transition metal cations are a very widespread technique to produce extended coordination polymers such as Metal-Organic Frameworks. In combination ... -
Vanadyl arsenates as catalysts for selective oxidation of organic sulfides and alkenes
Berrocal Torres, Teresa; Serrano Larrea, Edurne; Iglesias, Marta; Arriortua Marcaida, María Isabel (Elsevier, 2010-12-09)Two vanadyl arsenates templated with ethylendiamonium (EnVAs) and piperazonium (PipVAs) were evaluated as catalysts for the oxidation of thioethers and alkenes, using H2O2 and t-butyl hydroperoxide (TBHP) as oxidants. The ...